Surface modification of alginate sponge using tannic acid and dodecanethiol for diesel oil spill separation from water

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Ronald Wijaya, Kuan-Chen Cheng, Shella Permatasari Santoso, Shin-Ping Lin, Jindrayani Nyoo Putro, Jenni Lie, Chang-Wei Hsieh, Hsien-Yi Hsu, Alchris Woo Go, Artik Elisa Angkawijaya

2025 International Journal of Biological Macromolecules Vol. 317 Article Cited by 5 Quartile

Abstract

An environmentally friendly absorbent sponge was successfully developed for diesel spill remediation via alginate polymer crosslinking followed by surface modification using tannic acid and dodecanethiol (TA/Do). The optimal sponge was obtained with a 3 h crosslinking duration, achieving a balance between absorption performance and structural durability, while longer crosslinking times led to increased density and reduced efficiency. Surface modification imparted hydrophobicity to the alginate sponge, confirmed by a water contact angle of 120.2°, and the successful incorporation of TA/Do was confirmed from FTIR and XPS analysis. The modified sponge (AA-3-TA/Do) exhibited a diesel absorption capacity of 17.54 g/g—a 36 % increase over the unmodified form—and retained ∼90 % of this capacity after 34 absorption–desorption cycles. Kinetic modeling showed that diesel was rapidly absorbed during early contact, with faster uptake than water. A cytotoxicity assay confirmed its non-toxic nature, indicating environmental compatibility. This study demonstrates that a simple, scalable modification using accessible materials can significantly enhance oil sorbent performance without requiring complex techniques or hazardous reagents. © 2025 Elsevier B.V.

Affiliations

Chemical Engineering Department, National Taiwan University of Science and Technology, Taipei, 10607, Taiwan; Institute of Food Science and Technology, National Taiwan University, Daan District, Taipei City, 10617, Taiwan; Institute of Biotechnology, National Taiwan University, No. 1, Sec. 4, Roosevelt Rd., Taipei, Taiwan; Department of Optometry, Asia University, 500, Lioufeng Rd., Wufeng, Taichung, Taiwan; Department of Medical Research, China Medical University Hospital, China Medical University, 91, Hsueh-Shih Rd., Taichung, Taiwan; Department of Food Science, Fu Jen Catholic University, No. 510, Zhongzheng Rd., Xinzhuang Dist., New Taipei City, 242062, Taiwan; Chemical Engineering Department, Faculty of Engineering, Universitas Katolik Widya Mandala Surabaya, Jl. Kalijudan No. 37, East Java, Surabaya, 60114, Indonesia; Chemical Engineering Master Program, Faculty of Engineering, Universitas Katolik Widya Mandala Surabaya, Jl. Kalijudan No. 37, East Java, Surabaya, 60114, Indonesia; Collaborative Research Center for Zero Waste and Sustainability, Universitas Katolik Widya Mandala Surabaya, Jl. Kalijudan No. 37, East Java, Surabaya, 60114, Indonesia; School of Food Safety, Taipei Medical University, 250 Wu-Hsing Street, Taipei, 11031, Taiwan; Ph.D. Program in Drug Discovery and Development Industry, College of Pharmacy, Taipei Medical University, 250 Wu-Hsing Street, Taipei, 11031, Taiwan; Research Center of Biomedical Device, Taipei Medical University, 250 Wu-Hsing Street, Taipei, 11031, Taiwan; Department of Food Science and Biotechnology, National Chung Hsing University, South Dist, Taichung City, 402202, Taiwan; Department of Food Science, National Ilan University, Shennong Road, Yilan City, 260007, Taiwan; Department of Medical Research, China Medical University Hospital, Taichung City, 404333, Taiwan; School of Energy and Environment, Department of Materials Science and Engineering, Centre for Functional Photonics (CFP), City University of Hong Kong, Kowloon Tong, Hong Kong; Shenzhen Research Institute of City University of Hong Kong, Shenzhen, 518057, China; School of Engineering, University of San Carlos - Talamban Campus, Gov. M. Cuenco, Cebu City, 6000, Philippines; Center for Sustainable Resource Science, RIKEN, Yokohama, 230-0045, Japan